Laser Diffraction Masterclass 4 – How to Achieve Successful Method Transfer | Malvern Panalytical

Date recorded: May 30 2019

Duration: 42 minutes 25 seconds

In the fourth webinar of our Masterclass series, we will discuss how to achieve successful method transfer in three steps.

In many cases, the method transfer is straightforward and minimal work is required. But in regulated environments, for samples with more complex size distributions, or samples that are difficult to disperse, more work may be needed. Following the recommended process optimises the experiment matrix and maximises the likelihood of a sucessful method transfer.

Table of contents

1. Masterclass 4: Method transfer

01:32

2. Method transfer for laser diffraction

01:07

3. The pyramid of method transfer

01:54

4. The method transfer process

00:21

5. Information gathering

02:28

6. Information gathering

00:27

7. Information gathering

01:06

8. What is the biggest source of error?

00:38

9. What is the biggest source of error?

00:17

10. Information gathering

00:24

11. Information gathering

02:04

12. Experiments

04:09

13. Experiments

00:40

14. Analysis settings

02:55

15. Success criteria

00:26

16. Precision and accuracy

01:02

17. Precision and accuracy

01:18

18. Success criteria

01:43

19. Success criteria

01:25

20. Success criteria

01:18

21. Transferring methods from MS2000 to MS3000

00:12

22. Achieving comparable results

01:10

23. Experiments for method transfer

00:38

24. Obscuration

01:05

25. Achieving comparable wet dispersion

00:58

26. Obscuration filter and feed rate

00:49

27. Achieving comparable dry dispersion

00:35

28. Comparing pressure titrations

01:03

29. Analysis settings

00:49

30. Analysis: Optical properties

00:37

31. Analysis: Assessing the data fit

00:33

32. Analysis: Assessing the data fit

00:28

33. Analysis: Correct optical properties

00:18

34. Comparing results

00:55

35. Analysis: Mastersizer 2000 emulation

00:38

36. Slide 36

00:00

37. Summary

00:39

38. A six part series with 1 through 3 now available on-demand

00:22

39. Untitled

01:00

40. A six part series with 1 through 3 now available on-demand

01:01

41. Thank you for your attentionsarennah.longworth-cook@malvernpanalytical.com

00:19

42. Untitled

01:02

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