| 00:00:00 | Malvern’s Polyolefin Characterization Package Part II: |
| 00:01:26 | Malvern’s Polyolefin Characterization Package Part II: HT-DSV & FIPA-XS |
| 00:02:59 | Malvern Polyolefin Characterization Package: A Three Part Presentation |
| 00:03:25 | Malvern Polyolefin Characterization Package Part I HT-GPC Summary |
| 00:03:55 | Malvern Polyolefin Characterization Package Part I HT-GPC Highlights |
| 00:05:06 | Correlation of HT-GPC Data with Viscosity |
| 00:06:11 | HT-DSV Outline |
| 00:07:01 | What is Dilute Solution Viscosity (DSV)? |
| 00:07:48 | Traditional Measurement |
| 00:08:40 | Nomenclature for Solution Viscosity |
| 00:08:54 | Huggins/Kraemer Plot |
| 00:09:30 | Two Capillary Viscometer Principle |
| 00:10:29 | Poiseulle’s Law |
| 00:10:58 | How Does The Two Capillary Viscometer Work? |
| 00:11:04 | Baseline Condition |
| 00:11:42 | How Does The Two Capillary Viscometer Work? |
| 00:12:05 | Plateau Condition |
| 00:13:03 | Dilute Solution Viscometer (DSV) System |
| 00:14:11 | GPC / SEC Visual |
| 00:15:08 | Vortex Principle |
| 00:15:46 | Instrumental Setup |
| 00:16:00 | HT-DSV Experimental Conditions |
| 00:17:29 | Instrument Accuracy |
| 00:18:08 | Instrument Precision |
| 00:18:47 | Instrument Precision |
| 00:19:14 | Instrument Precision |
| 00:19:48 | Sample Homogeneity Problem |
| 00:20:10 | Sample Homogeneity Problem |
| 00:21:13 | IV vs MFI Correlation |
| 00:21:38 | Untitled |
| 00:21:45 | Untitled |
| 00:21:55 | Untitled |
| 00:23:04 | FIPA-XS Outline |
| 00:23:57 | Complete Triple Detector GPC Instrument: OmniSEC Software Control |
| 00:24:14 | Triple/Tetra Detector Array (TDA) |
| 00:24:22 | Flow Injection Polymer Analysis (FIPA) |
| 00:24:45 | Separation Techniques |
| 00:26:24 | What is FIPA? |
| 00:26:47 | Industrial Application of Light Scattering and Viscometry |
| 00:27:55 | Selection of FIPA Applications |
| 00:28:16 | Xylene Soluble of Polyolefins |
| 00:29:32 | Traditional Gravimetric vs Malvern FIPA Xylene Soluble Methods |
| 00:31:27 | Triple FIPAGram of EPR Xylene Soluble Fraction |
| 00:31:44 | FIPA Data for EPR Xylene Soluble |
| 00:32:46 | Reproducibility of FIPA-XS 3 Operators & 3 FIPA Instruments |
| 00:34:43 | Correlation of FIPA vs Gravimetric |
| 00:35:06 | Summary of XS Techniques |
| 00:41:19 | Conclusions |
| 00:43:01 | Contact Information |
Firstly results presented in Part 1 of this three part polyolefin series are reviewed. Secondly how high temperature dilute solution viscosity (DSV) and Xylene Solubles (XS) techniques complements HT-GPC for the analysis of polypropylene