Pushing the Limits of X-Ray Powder Diffraction in the Laboratory | Malvern Panalytical

Date recorded: December 03 2019

Duration: 43 minutes 38 seconds

Typically, the reference for high resolution and high intensity in powder diffraction is the use of the synchrotron radiation. However getting access to such large scale facilities might be a tedious task and definitively not as often as one would like. Consequently, it is important to know how far one can push the limits of a powder diffraction in the laboratory. Using various examples of materials, from perovskite materials, to permanent magnets or mineralogical related materials; we will review what can be done in the laboratory and see how it can compete with synchrotron radiation in some instances.

Table of contents

1. Pushing the limits of X-ray powder diffraction in the laboratory

02:47

2. Table of content

00:36

3. When high resolution matters: Cu Ka1 reveals subtle structural changes in MnBi

00:09

4. When high resolution matters: Cu Ka1 reveals subtle structural changes in MnBi

00:32

5. When high resolution matters: Cu Ka1 reveals subtle structural changes in MnBi

00:59

6. When high resolution matters: Cu Ka1 reveals subtle structural changes in MnBi

00:27

7. When high resolution matters: Cu Ka1 reveals subtle structural changes in MnBi

01:01

8. When high resolution matters: Cu Ka1 reveals subtle structural changes in MnBi

01:10

9. Do you always need synchrotron radiation?

00:14

10. Structural phase transitions in EuNbO3 perovskite

00:40

11. Structural phase transitions in EuNbO3 perovskite

01:06

12. Laboratory X-ray data: Cu Ka data

00:17

13. Laboratory X-ray data: Cu Ka data

00:45

14. Laboratory X-ray data: Cu Ka data

00:17

15. Empyrean Alpha-1

00:21

16. Octahedral tilting: Imma

00:49

17. Comparison synchrotron Vs. laboratory

01:09

18. Comparison synchrotron Vs. laboratory

00:44

19. Comparable resolution between synchrotron and laboratory

00:14

20. CrF3.3H2O: reported crystal structure

00:40

21. CrF3.3H2O: Cu Ka1 data

00:13

22. CrF3.3H2O: Cu Ka1 data

00:23

23. Comparison synchrotron Vs. laboratory

00:53

24. Comparison synchrotron Vs. laboratory

00:48

25. Comparison synchrotron Vs. laboratory

01:26

26. Crystallography with Bragg-BrentanoHD

00:13

27. LiCrGe2O6: P21/c versus C2/c

01:17

28. LiCrGe2O6: P21/c versus C2/c

00:28

29. LiCrGe2O6: P21/c versus C2/c

00:34

30. LiCrGe2O6: real symmetry P21/c

00:36

31. When you are too soft, try harder!

00:14

32. From customer support to scientific collaboration

00:19

33. How did it begin?

00:35

34. Kalistrontite: a rare mineral

00:33

35. Kalistrontite: a rare mineral ?

00:26

36. Solving the structure of Kalistrontite

00:51

37. Solving the structure of Kalistrontite

00:55

38. Solving the structure of Kalistrontite

00:28

39. Why to use hard radiation ( = Mo) for diffraction?

01:21

40. Solving structure with hard radiation

01:12

41. Solving structure with hard radiation

00:31

42. Solving structure with hard radiation

00:32

43. Solving structure with hard radiation

00:50

44. Solving structure with hard radiation

00:27

45. New article

00:14

46. Other articles using structure solution from powder data using Malvern Panalytical technology

00:23

47. Conclusion

00:04

48. Conclusion

01:41

49. Acknowledgements

00:05

50. Acknowledgements

00:42

51. Questions and Thank You!

09:27

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