ASD LabSpec 4 Hi-Res analytical instrument

Superior spectral resolution for sharp feature recognition

  • 3 nm VNIR, 6 nm SWIR spectral resolution
  • Covers full 350-2500 nm spectral range
  • High analytic throughput rates

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Overview

The ASD LabSpec 4 Hi-Res analytical spectrometer is designed for analysis of materials that are characterized by sharp spectral features that may require more resolute spectral data for accurate detection and identification.

The LabSpec 4 is optimized for rapid analysis and is ideal for fast-moving laboratory environments, providing instant results with no sample preparation. 

  • Evaluate hundreds of samples per day with high analytic throughput rates
  • Identify spectral characteristics of both liquids and solids in real-time
  • Non-destructive measurement means no sample preparation and allows for the reuse of the sample in other research
  • Measure multiple properties simultaneously through NIR energy that penetrates several millimeters into organic substances
  • Rapid analysis moves with the speed of production to evaluate incoming, in-process, or finished materials almost instantaneously
  • Compatible with all ASD sampling accessories

Features

  • Best for: users requiring maximum sensitivity, ideal for outdoor and remote sensing applications.

  • Cost-effective alternative: provides a lower-cost solution for those not requiring FieldSpec’s high-end performance.

  • Artificial light advantage: a lower signal-to-noise ratio can be compensated for with powerful artificial light sources.

  • User-replaceable fibre optic cable: features SMA 905 connector for easy cable replacement and flexible light source options.

Superior spectral performance

The 3 nm VNIR, 6 nm SWIR spectral resolution of the LabSpec 4 Hi-Res provides superior performance across the 350-2500 nm spectral range. The enhanced spectral resolution in the SWIR range (1001-2500 nm) is particularly useful for detecting and identifying compounds with narrow spectral features in these longer wavelengths such as soil, mineralogy, pharmaceuticals, cosmetics, plastics and petrochemicals

Spectral data with 6 nm SWIR resolution provides a strong foundation for building accurate chemometric calibration models for quantitative and qualitative materials analysis. The spectrometer configuration delivers superior signal throughput and is compatible with all ASD bifurcated probes and lighted accessories.

Optional integrated fiber optic light source

The ASD LabSpec 4 Hi-Res i model includes an internal broad-spectrum halogen light source that eliminates the need for an external fibre optic light source, which is required for bifurcated probes and some accessories.

Why post-dispersive technology matters

Pre-dispersive systems: Disperse light before reaching the sample, relying on an internal light source.

Post-dispersive systems: Disperse light after reflection, allowing external light sources like the sun to be used.

The post-dispersive system technology used in ASD instruments offers superior analysis capabilities:

  • Measures reflected energy from external light sources
  • Adapts to different lighting conditions without internal light dependence
  • Provides reliable calibration for spectral radiometry

Key applications

Plant Physiology

ASD systems are used to determine plant physiological status, including disease status, nutritional status related to nitrogen uptake and moisture balance.

Pharmaceuticals
  • Rapid, accurate measurement of constituents and product purity in pharmaceuticals products where and when it’s needed.
  • Pharmaceutical Analysis and Quantitative Chemical Analysis: When you require rapid, accurate measurement of pharmaceutical products, look no further than ASD’s complete line of Vis/NIR spectrometers.
Forest products and pulp and paper analysis

In recent years, the forest products industry has issued an increasing call for process measurement innovation to reduce cost and increase profitability. ASD has answered.

Counterfeit drug detection

ASD has a truly mobile pharmaceutical anti-counterfeit solution to help combat this problem with the LabSpec NIR spectrometer.

Quality control and raw material analysis

Cost-effective rapid, real-time determination of the constituents and purity of raw materials for a multitude of industries.

Precision agriculture
  • From the field to the processing plant, agricultural product intended for widespread food consumption must meet numerous international quality standards.
  • Grain and Seed Analysis: Proper characterization of grain and seed quality is critically important for germplasm development, grain collection and grain processing.
Moisture analysis

For cost-effective and rapid, non-destructive, in-situ moisture concentration analysis in a wide range of materials and concentrations.

Plastics and plastic films

Qualification and quantification of raw material prior to introduction into a production process and analysis of in-process materials and finished products in the industrial plastics industry.

Food
  • General food analysis: Rapid, non-destructive and in-situ analysis of fat, protein, moisture, sugar, brix and acidity levels for the food, beverage, and dairy industry.
  • Nutraceuticals and Dietary Supplements: Cost-effective and non-destructive material inspection and analysis to assist natural product and supplement manufacturers meet new FDA regulations for the standardization and purity of ingredients.
Cosmetics and beauty products

Rapid in-situ analysis of the purity and chemical composition present in raw materials, in-process materials, and finished product for the cosmetics and beauty products industry, including evaluation of color value for hair dye.

Biomass and biofuels analysis

From characterization of oil content of soybeans and other crops, to quantification of key parameter levels in biofuel processing and quality analysis of final product, near-infrared (NIR) spectroscopy is the ideal measurement tool.

Specification

Spectral performance 350-2500 nm
Resolution
3 nm @ 700 nm
6 nm  @ 1400/2100 nm
Measurement time 100 milliseconds
Signal-to-noise ratio
VNIR 9,000:1 @ 700 nm
SWIR 1 9,000:1 @ 1400 nm
SWIR 2 4,000:1 @ 2100 nm
Noise
VNIR 4.8 x 10-5 AU or 48 μAU@ 700 nm
SWIR 1 4.8 x 10-5 AU or 48 μAU@ 1400 nm
SWIR 2 1.1 x 10-4 AU or 110 μAU@ 2100 nm
Detector
(350-1000 nm) 512 element silicon array
(1001-1800 nm) & (1801-2500 nm) Graded Index InGaAs Photodiode, TE Cooled
Regulatory testing
CE certified EN61010-1:2001 2nd Edition 
CE certified EN61326-1:2013
EU Directive 2006/95/EC, 2004/108/EC
Calibration type
NIST traceable calibration 21 CFR Part 11 - installed per customer request
USP 1119 - installed per customer request and purchase of applicable USP Standards
Communication port
Wired 10/100 Base T Ethernet port with Ethernet cross-over cable                      
Wireless 802.11g/n wireless card
Dimensions 12.7 x 36.8 x 29.2 cm (5 x 14.5 x 11.5 in)
Weight 5.44 kg (12 lbs)
Power
AC/DC switching power supply or a sealed lead-acid gel battery
AC input 90-240 VAC, 50/60 Hz
DC input 12 VDC, 60 W
Auxiliary port power: output, +12 VDC, 27 Watt (max)
Software Indico® Pro, GRAMS spectroscopy software suite by Thermo Scientific, The Unscrambler® by Camo Software
Warranty One year full warranty including expert customer support
Computer Windows® 10 64-bit laptop (instrument controller)

Accessories

Probes and Lighting

Contact Probe

The ASD Contact Probe is designed for contact measurements of solid raw materials such as minerals, grains, other granular materials. Its innovative optical design minimizes measurement errors associated with stray light and allows for the measurement of samples through clear and transparent plastic bags.

In addition to the standard contact probe, we also offer the Hi-Brite contact probe and the Plant Probe.

All contact probes are available with a ruggedized cable feed and cable, designed for applications that involve extra cold or harsh temperatures.

Length 10" ( 25.4 cm)
Weight 1.5 lbs (.7 kg)
Power requirements 12-18 VDC, 6.5 W
Lightsource type/Life (approx.) Halogen bulb/1500 hours
Halogen bulb color temperature 2900 K
Spot size 10 mm
Contact Probe

Rapid analysis probe

The Rapid Analysis Probe is specifically designed for speedy spectral collection of powders and other fine-grained materials such as small uniform seeds and grains. Its beveled tip and metal jacket greatly speed up the spectral collection process of fine-grained materials to optimize workflow. Simply insert the Rapid Analysis Probe into your fine-grained media, collect the spectrum, use a chemical wipe to swipe the probe clean and move on to the next sample. It’s that easy! The Rapid Analysis Probe comes with a gimbaled white reference for high-performance calibration. It can be used for quantitative predictive models.

If using this probe with a spectrometer such as a TerraSpec mineral analyzer or a LabSpec lab analyzer without an integrated light source, a Fiber Optic Illuminator is necessary. The Fiber Optic Illuminator provides the light source needed for sample collection.

Technical Specifications

  • Length: 21.6 cm (8.5 inches)
  • Spot size: 4 mm
Rapid analysis probe

Small diameter reflectance probe

With an approximate spot size of only 2 mm, the Small Diameter Reflectance Probe was designed to collect spectra from individual small materials such as individual grains or vugs in a hand sample or rock core. It’s perfect for determining specific mineralogy of individual grains.

If using a spectrometer such as a TerraSpec mineral analyzer or a LabSpec lab analyzer without an integrated light source, a Fiber Optic Illuminator is required. The Fiber Optic Illuminator provides the necessary light source for sample collection.

Technical Specifications

  • Length: 10.2 cm (4 inches)
  • Field of View: 1 mm
Small diameter reflectance probe

Muglight

The ASD Muglight is designed for analysis of raw materials requiring reflectance and absorbance measurements. It can measure samples through glass vials, or using the ASD sampling tray adapter. It's unique and innovative design minimizes measurement errors associated with stray light and specular reflected components. 

For users requiring higher intensity illumination, ASD also offers the Hi-Brite Muglight.

Size 5.5” x 3.7” (14cm x 9.4cm)
Weight 2.91 lbs (1.3 kg)
Power requirements Input power 5.5 W, bulb 4 W
Light source (type/life) approx. Tungsten Quartz Halogen b/1500rs
Bulb color temp 2900 K
Spot size 12 mm
Muglight

Integrating Sphere

Integrating spheres collect reflected light from samples over a full hemisphere. The sphere, by nature of its internal diffuse (lambertian) reflection and integration of the energy, is insensitive to directional reflectance features coming from the sample, and therefore, gives a very repeatable “averaged” response to the reflectance of the sample placed in the beam at the sphere port. 

Sample placement and incidence beam/collection alignment are less critical to the measurement results because the integrating sphere looks at representative averaged energy from all angles at the same time.

Configurable in a number of different ways, with very minimal set up, the sphere allows for rapid analysis of several important quantities:

  • 13º/D Total Hemispherical Reflectance (Specular Included)
  • Comparison Method and Substitution Method
  • 13º/D Hemispherical (Specular Excluded) Reflectance Factor
  • Normal Hemispherical Transmittance
Integrating Sphere

Turntable

When your application requires analysis of irregularly shaped or non-homogeneous samples, the ASD Turntable is ideal for obtaining a highly accurate average. 

Especially useful for instrument owners in the grain, agriculture, pulp and paper, food, plastics and mining industries.

  • 53.2 mm sampling spot size
  • Rotates at 22 RPM
  • Fits up to a 150mm sample dish
  • Compact (8"x11"x11" or 20.32 cm x 27.94 cm x 27.94 cm) footprint.

The Turntable comes standard with a 4000 hour halogen light source and one standard 150 mm x 15 mm Petri dish.

Turntable

Fiber optic illuminator

The Fiber Optic Illuminator is a portable, external light source designed for use with ASD instruments and sampling accessories that do not have a built-in light source.

Length 11.43 cm (4.5 inches)
Width 8.255 cm (3.25 inches)
Weight 292 grams (10.3 ounces)
Fiber optic illuminator

General

goLab mobile work station

Now, technicians and researchers, armed with a powerful ASD spectrometer system and the goLab Mobile Work Station, are more empowered than ever before to take the lab to the sample location, and easily perform analyses formerly restricted to a laboratory environment.

The goLab Mobile Work Station acts as a wheeled carrier for streamlined transport between locations, and then quickly unfolds to support all your sampling needs right on the spot.

The goLab Mobile Work Station Features:

  • Large wheels for easy transport
  • Stable, non-slip platform for spectrometer, sampling probe, and computer
  • Convenient and secured compartments for batteries and accessory kit
  • Compatible with all current ASD portable spectrometer systems
  • Folds down for compact storage and transport
  • Ideal for both inside and outside work
  • Reconfigurable velcro positioning for added flexibility
goLab mobile work station

Reference Panels

ASD carries a wide array of calibrated and non-calibrated diffuse white and gray reference panels in varying sizes (from 2 x 2 in. to 12 x 12 in. or 5.1 x 5.1 cm to 30.5 cm x 30.5 cm) and reflectance levels, including encapsulated gray scale (NIST/NRC traceable) wavelength and USP standards for USP 1119. Calibrated panels come with certificate and documentation showing standard deviation and reflectance factors.

All reference panels and standards may be purchased separately. To provide our customers with a more cost-effective approach, specific sizes or styles of reference panels are included in accessory bundles designed for maximum compatibility with a particular application.

Your ASD sales representative will be able to advise you on the best option(s) for your needs.

Reference Panels

Palm grip

Optional palm grip with bare fiber optic input:

  • Secures the fiber optic cable during fieldwork
  • Prevents damage from unexpected tension
  • Ensures consistent lighting conditions during measurements
Palm grip

Telescopic tubes

A variety of telescopic tubes are available for long-range measurements:

  • 1-degree fore optic: measures distant objects up to 100 feet away
  • Smaller telescopic tubes: focus on specific areas within 10 feet
  • Spot Size Matching: ensures accurate data by aligning the instrument field of view with satellite pixel resolution
Telescopic tubes

User manuals

Software downloads

24 August 2017

6.5.6.1

Indico Pro
6.5.6.1

24 August 2017

6.5.6.1

LabSpec 4 Software Installation
6.5.6.1

23 June 2016

6.40

Wavelength Verification ASD Puck 8 nm Resolution
6.40

23 October 2017

6.40

Wavelength Verification ASD Puck 6 nm Resolution
6.40

07 June 2016

4.0.1

Instrument Configuration v4.0.1
4.0.1

16 August 2016

1.20

Dark Current calibration
1.20

Support

Services

Solutions to maximize the return on your investment

To assure that your instrument remains in top condition and performs on the highest level, Malvern Panalytical offers a wide range of services. Our expertise and support services assure an optimal functioning of your instrument.

Support

Service for a lifetime

  • Phone and remote support
  • Preventive maintenance and checkups
  • Flexible Customer Care Agreements
  • Performance certificates
  • Hardware and software upgrades
  • Local and global support

Expertise

Adding value to your processes 

  • Sample preparation development/optimization
  • Analytical methodologies 
  • Turnkey solutions for XRD 
  • Operations via IQ/OQ/PQ, quality assurance (GLP, ISO17025) or round robins/inter laboratory studies
  • Consultancy services

Training and education

  • Training on-site or at our competence centers
  • Broad range of basic and advanced courses on products, applications and software
Superior spectral resolution made easy.

Superior spectral resolution made easy.

Designed for analysis of sharp spectral features, the LabSpec 4 Hi-Res offers more resolute spectral data for accurate detection and identification.

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