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Mastersizer 3000E

Entry level particle size analyzer

The Mastersizer 3000 is highly regarded as the premier laser diffraction particle size analysis instrument on the market for design, performance and software user experience. However, some customers do not immediately need the advanced functionality that the Mastersizer 3000 offers. Malvern Panalytical have therefore introduced an entry level instrument to the Mastersizer product family which is based upon the proven design of the Mastersizer 3000 but with more basic performance and software functionality.

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Overview

The Mastersizer 3000E provides a cost-effective, entry level particle sizing system which can be upgraded as required. It is available with two different performance levels:

Mastersizer 3000E Basic

  • Particle size range from 0.1 – 1000µm
  • Manual dispersion units only
  • Basic software, with updates and bug fixes only
  • Anytime upgrade option to Mastersizer 3000E Extended

Mastersizer 3000E Extended

  • Automated wet sample dispersion units supported
  • All the advanced software functionality offered with the Mastersizer 3000, including updates, bug fixes and upgrades

How it works

The Mastersizer 3000E uses the technique of laser diffraction to measure the size of particles. It does this by measuring the intensity of light scattered as a laser beam passes through a dispersed particulate sample. This data is then analysed to calculate the size of the particles that created the scattering pattern.

A typical system is made up of three main elements:

  • Optical bench - A dispersed sample passes though the measurement area of the optical bench, where a laser beam illuminates the particles. A series of detectors then accurately measure the intensity of light scattered by the particles within the sample over a wide range of angles.
  • Sample dispersion units (accessories). Sample dispersion is controlled by a range of wet and dry dispersion units. These ensure the particles are delivered to the measurement area of the optical bench at the correct concentration and in a suitable, stable state of dispersion.
  • Instrument software. The Mastersizer 3000E software controls the system during the measurement process and analyzes the scattering data to calculate a particle size distribution.

Specification

General

Particle size Suspensions, emulsions, dry powders
Principle Laser light scattering
Analysis Mie and Fraunhofer scattering
Data acquisition rate 10 kHz
Typical measurement time <10 sec
Dimensions (W, D, H) 690mm x 300mm x 450mm
Weight 30 kg

Optics

Red light source Max. 4mW He-Ne, 632.8nm
Blue light source None
Lens arrangement Reverse Fourier (convergent beam)
Effective focal length 300mm

Detector

Arrangement Log-spaced array
Angular range 0.032 - 60 degrees
Alignment Automatic

Size

Particle size 0.1 - 1000 µm *
Number of size classes 100 (user adjustable)
Accuracy Better than 0.6% **
Precision / Repeatability Better than 0.5% variation *
Reproducibility Better than 1% variation *

System compliance

Laser safety Class 1, IEC60825-1:2007 and CFR Chapter I: Sub-chapterJ: Part 1040 (CDRH)
Regulatory testing RoHS and WEEE compliant CE / FCC compliant Meets requirements of the European Low Voltage directive

System

Power 100/240 v, 50/60 Hz 50W (no dispersion units connected) 200W maximum (2 dispersion units connected)
Humidity 80% maximum for temperatures up to 31°C, decreasing linearly to 50% at 40°C. Non condensing.
Product storage temperature -20°C to +50°C
Ingress Protection (IP) rating IP41B
Operating temperature (°C) +5°C to +40°C

Notes

* Sample and sample preparation dependent.
** Accuracy defined for the recovery of the mean size of a narrow log-normal distribution. Sample and sample preparation dependant.
Patents The Mastersizer 3000E optical bench is protected by patent GB2,340,932; together with patents based on applications WO2013038161 and WO2013038159. Hydro MV and LV protected by EP1167946A2 and related filings.

Accessories

Sample dispersion accessories for the Mastersizer 3000E

Mastersizer 3000E Basic and Extended

Hydro Insight

A window into deeper materials analysis

The Hydro Insight is a dynamic imaging accessory that sits alongside the Mastersizer 3000, providing insights that go beyond particle size distribution to particle images and quantitative particle shape data. 

In this way, it helps scientists, researchers, and quality-control managers understand their materials better, develop methods faster, and simplify troubleshooting.

Hydro SV

Small volume wet sample dispersion

The Hydro SV is a simple, cost effective liquid dispersion unit designed to enable particle size analysis using small volumes of sample and dispersant.

Hydro EV

Flexible volume wet dispersion

A unique dip-in wet sample dispersion unit that can be used with standard laboratory glassware. Suitable for a wide variety of dispersant volumes and particle size ranges.

Hydro SM

Small volume entry level wet dispersion unit

The Hydro SM is a cost effective wet sample dispersion unit designed for measuring samples in non-aqueous dispersants where solvent usage needs to be minimized.

Aero M

Routine particle size analysis for bulk dry powder samples

The Aero M dry powder disperser enables bulk dry powder samples to be measured using the Mastersizer 3000E laser diffraction particle size analyzer. Its simple design ensures that it is easy to use and maintain, delivering robust, reproducible particle size distribution measurements as part of routine production or quality control operations.

Aero Funnel Sample Feeder

Rapid QC measurements for bulk powder samples

The Aero funnel sample feeder is designed to help users achieve rapid, reproducible bulk dry powder particle size measurements by allowing samples to be added directly to the Aero S and Aero M dry powder dispersion units without opening the dispersion unit lid. This speeds up and simplifies the process of introducing samples for analysis, decreasing the time required to obtain results.

Mastersizer 3000 Chocosizer

Effective Chocolate production quality control

The goal of chocolate production is to produce a product with a consistent taste and mouthfeel in an economical and efficient way. Control of the cocoa and milk solids particle size and particle size distribution is critical to achieving this objective. The Mastersizer 3000 Chocosizer is designed to support chocolate production and quality control by providing a simple method for fast, reliable chocolate particle size analysis.

Mastersizer 3000E Extended only

Hydro MV

Medium volume automated dispersion unit.

The Hydro MV is a medium volume unit for the controlled, automated wet dispersion of samples for particle size analysis. Suitable for both aqueous and non-aqueous applications, it is especially useful when sample size is limited and/or dispersant use must be minimized.

Hydro LV

Large volume wet sample dispersion.

The Hydro LV is an automated large volume unit that controls wet dispersion of materials for particle size analysis. It is especially suitable for applications where the sample size is relatively large or the size distribution is very broad.

Support

Protect your investment and ensure optimized performance at all times with Malvern Panalytical's service plans.

When you purchase a Malvern Panalytical product we understand that this is just the first stage of a working relationship that will last for the lifetime of the instrument. Depending on your needs, Malvern Panalytical will provide the support for your business.

Help Desk

Training

  • User training events

Software downloads

Malvern Panalytical's service options- choose the right plan for you:

Malvern Panalytical Platinum Plan

For laboratories where maximizing instrument up-time is critical to its daily performance. Our highest level of response and the 'all inclusive' price plan takes care of those unexpected repair bills should the unfortunate occur.

Malvern Panalytical Gold Plan

Enhance your laboratory productivity by maintaining instrument efficiency. Still receive that priority response, combined with specialist technical and software support, we'll keep your instrument performance on track to deliver.

Malvern Panalytical Bronze Visit

For laboratories looking to optimize instrument performance, regular preventative maintenance is essential.

Platinum PlanGold PlanBronze Visit
Annual PM/PV Test
yes
yes
no
Telephone / Email Support
yes
yes
no
Priority Response
yes
yes
no
Emergency Breakdown visits*
yes
yes
no
Parts Included
yes
no
no
Technical & Software Support
yes
yes
yes
IQ/OQ (Pharma)***
yes
yes
yes

*including labour & travel costs ***available at an additional cost

It can accurately measure commercial standards which satisfy our ISO initiatives and provides great confidence on the data we collect for our clients

Carlos Eyzaguirre — FLSmidth