Civil engineering, architecture, and archaeology

Find out how our solutions can advance your civil engineering, architecture, and archaeology knowledge

Interested in how our analysis methods can benefit your civil engineering, architecture, or archaeology research? Whether you’re a student, a researcher, or a professor, we’ve put together some links to the most relevant application examples.

The materials researched and analytical equipment used in civil engineering and architecture often overlap with Chemistry and Applied Chemistry, and Materials Science and Engineering – so feel free to check out those pages for more information! Method abbreviations are explained at the bottom of this page.

Archaeological materials

The study of archaeological materials typically includes:

  • Mineral chemistry for glasses, pottery, and pigments
  • Metallurgy for coins and metallic artifacts
  • Knowledge of all types of building materials


Here’s a selection of application notes and articles related to the study of Archaeological materials. Check them out to discover more!

Archaeological Materials      

Method

Sample

Application Note Title (Link)

Coins - metal composition

XRF

Archeological coin

Practical small spot mapping. Analysis of an archeological coin using SumXcore technology

Mortar - composition

UV/Vis/NIR/ SWIR

Mortar in walls of Ruins of Pompeii, Italy

Portable Analysis of Ancient Walls in Pompeii, Italy

Paints - Identification

UV/Vis/NIR/ SWIR

Medieval and Renaissance illuminated manuscripts (10th-16th century)
 in the collection of the Fitzwilliam Museum in Cambridge, UK

Report on the Use of a FieldSpec 4 Spectroradiometer for the Non-Invasive Identification of Artists' Materials on Illuminated Manuscripts

Paints - mineral compositions

XRD

Chemical and mineralogical changes to a wall painting in the St George fresco, Prague, Czech Republic
cerussite, plattnerite, lead magnesium carbonate, calcite, hydrocerussite

X-ray micro-diffraction in wall painting research

Paints – mineral compositions

XRD

Study of pigments in a medieval parchment leaf using microdiffraction

Non-destructive, small-scale analysis of cultural heritage objects with Empyrean

Building materials

In order to demonstrate compliance with building regulations and materials standards, both civil engineers and architects must have a strong understanding of their building materials, including:

  • Materials science
  • Mechanical properties
  • Chemistry
  • Processing requirements


Understanding of pre-manufacturing processes is also an important element in the drive to create building materials with a lower CO2 footprint. 

Take a look at the application notes below for examples of how our solutions can help with this!

Building Materials

Method

Sample

Application Note Title (Link)

Adhesives - resin loading in wood

UV/Vis/NIR/ SWIR

Resin loading in wood, wood adhesives, resin, wax, and moisture in OSB chips

Wood Adhesives Presentation

Architectural marble fillers - particle size

LD

Marble Fillers/ calcium carbonate

Automated marble milling - better product quality, lower energy costs

Asphalt emulsions - particle size, Zeta potential

LD / DLS / ELS

Asphalt emulsions (asphalt cement, water, emulsifier, additives)

Determining the quality of asphalt emulsions using particle size and zeta potential analysis

Cement - accurate elemental analysis

XRF

Cement (SiO2, Al2O3, Fe2O3, CaO, MgO, SO3, K2O, Na2O, TiO2, P2O2, ZnO, Mn2O3)

Zetium - Cement analysis using CEMOXI standards

Cement - accurate elemental analysis

XRF

Cement (SiO2, Al2O3, Fe2O3, CaO, MgO, SO3, K2O, Na2O, TiO2, P2O2, ZnO, Mn2O3)

Analysis of major and minor elements in cement pressed powders

Cement - elemental analysis compliance with industry norms

XRF

Cement (SiO2, Al2O3, Fe2O3, CaO, MgO, SO3, K2O, Na2O, TiO2, P2O2, ZnO, Mn2O3)

Zetium - Compliance made easy ASTM C114-13 norm

Cement - elemental analysis compliance with industry norms

XRF

Cement (SiO2, Al2O3, Fe2O3, CaO, MgO, SO3, K2O, Na2O, TiO2, P2O2, ZnO, Mn2O3)

Compliance made easy and faster - ASTM C114-15 norm with SumXcore at 1 kW

Cement - elemental analysis compliance with industry norms

XRF / SPE

Cement (SiO2, Al2O3, Fe2O3, CaO, MgO, SO3, K2O, Na2O, TiO2, P2O2, ZnO, Mn2O3)

ASTM C114-15 and ISO 29581-2 compliance for cement fused beads in 10 minutes

Cement - sample preparation and elemental composition

XRF / SPE

SiO2, Al2O3, Fe2O3, CaO, MgO, SO3, K2O, Na2O, TiO2, P2O5, ZnO and Mn2O3 in cement

ASTM C114-15 and ISO 29581-2 compliance for cement fused beads

Cement - sample preparation for XRF

SPE

Cement powder, lithium borate

Cement XRF application using a universal borate fusion methodology for ASTM C 114 & ISO/DIS 29581-2 qualification

Cement and Clinker Powders - particle shape and size

MDRS

Clinker and cement powders

Component-specific characterization of cements using Morphologi ID

Cement Blending - mineralogical composition

XRD

Blended cement

Quick mineralogical quantification of blended cement

Cement finishing - particle size

LD

Cement finishing

Reducing the cost of cement production through the use of automated process control

Cement manufacture - CO2 reduction by accurate process control

XRD

Clinker and cement

Quick phase quantification of clinker and cement for environmentally friendly cement production

Cement manufacture - on-line particle sizing

LD

Cement grains

On-line particle sizing and control

Cement manufacture - on-line particle sizing

LD

Cement grains

Castles' on-line analysis- article

Chlorine in Cement - Sample Preparation for XRF

SPE

Chlorine in Cement

Analysis of Chlorine in Cement and Cement Related Materials Using Borate Fusion and XRF Analysis

Chlorine in concrete - concentration

UV/Vis/NIR/ SWIR

Chlorine in Concrete (raw material and bridge constructions)

Determination of chloride ion concentrations in concrete by means of near-infrared spectrometry

Chromium in cement - crystalline phase analysis

XRD

Chromium phases in cement

Measurement of fast reactions. Chromium in cement - measuring the kinetics of lamellar calcium aluminate chromate hydrates

Clinker - crystalline phase analysis

XRD

Clinker phases, slag, fly ash, pozzolan

Cluster analysis

Clinker - sample preparation for XRD

XRD

Clinker: Alite, Belite, Free Lime (CaO), Ferrite, Aluminate,

Sample preparation of clinker

Clinker grinding - particle size

LD

Ground Clinker (Portland Cement, Raw Mix, calcium oxide, silicon oxide, aluminum oxide, ferric oxide and magnesium oxide, clay, limestone + Calcium Sulphate)

Particle size analysis of cement using the technique of laser diffraction

Clinker hydration kinetics - crystalline phase analysis

XRD

Clinker phases, minor phases - process of carbonization and hydration

Transmission geometry for Cement hydration kinetics

Clinker manufacture - polymorph identification

XRD

M1 and M3 Polymorphs of Alite in Clinker

Quantification of the M1 and M3 polymorphs of alite in OPC clinker

Clinker Manufacture, Raw Mix - elemental composition

XRF

Na2O, MgO, Al2O3, SiO2, SO3, Cl, K2O, CaO, TiO2, and Fe2O3 in raw mix

Fast raw mix analysis in compliance with GB/T19140-2003 and GB/T176-2008

Clinker Manufacture, Raw Mix - elemental composition

XRF

MgO, Al2O3, SiO2, SO3, Cl, K2O, CaO, TiO2, and Fe2O3 in raw mix,

Economical raw mix analysis in 5 minutes

Clinker manufacture, Raw Mix - sample preparation for XRF

SPE

Cement powder, lithium borate

Raw materials XRF application for the cement industry using a universal borate fusion methodology

Concrete - crystalline phase analysis, porosity, density

XRD - CT

Concrete

X-ray analysis of concrete: A multi-dimensional investigation using X-ray diffraction and computed tomography

Concrete - porosity measurement

CT

Porous Concrete

CT measurements with GaliPIX3D

Fly ash - routine elemental analysis

XRF

Coal fly ash, calcium hydroxide (from Lime, or Portland cement)

Zetium - Routine analysis of coal fly ash

Fly ash and slag additives - crystalline phase analysis

XRD

Replacement of Ordinary Portland Cement (OPC) by partially supplementing Clinker with fly ash and slag

XRD analysis of hydrated cements and cementitious systems

Mortar - elemental composition

XRF

Mortar: Ca, Si, Al, Fe, Na, K, Mg, S, Ti, Sr in Cement Paste

Examine reaction kinetics of mortar about 100 times faster with HiPer small spot mapping

Abkürzungen erklärt

Unsere Produkte und Technologien werden auf den Produktseiten beschrieben. Nachstehend finden Sie eine Kurzübersicht über die von unseren Geräten gemessenen Eigenschaften einschließlich der Messbezeichnung und ihrer Abkürzung. Klicken Sie auf die einzelnen Methoden, um mehr darüber zu erfahren! 

Abkürzung

Methodenname

Gerät(e)

Gemessene Eigenschaft

DLS

Dynamische Lichtstreuung

Zetasizer

Molekülgröße, hydrodynamischer Radius RH, Partikelgröße, Größenverteilung, Stabilität, Konzentration, Agglomeration

ELS

Elektrophoretische Lichtstreuung

Zetasizer

Zetapotenzial, Partikelladung, Suspensionsstabilität, Proteinmobilität

ITC

Isothermische Titrationskalorimetrie

MicroCal ITC

Bindungsaffinität, Thermodynamik molekularer Reaktionen in Lösung

DDK

Dynamische Differenzkalorimetrie

Microcal DSC

Denaturierung (Entfaltung) von großen Molekülen, Stabilität von Makromolekülen

GCI

Gittergekoppelte Interferometrie

Creoptix WAVEsystem

Bindungskinetik und -affinität in Echtzeit, markerfrei mit Fluidik

IMG

Automatisierte Bildanalyse

Morphologi 4

Bildgebung von Partikeln, automatisierte Form- und Größenmessung

MDRS

Morphologically-Directed Raman-Spektroskopie

Morphologi 4-ID

Bildgebung von Partikeln, automatisierte Form- und Größenmessung, chemische Identifizierung und Verunreinigungserkennung

LD

Laserbeugung

Mastersizer

Spraytec

Insitec

Parsum

Partikelgröße, Größenverteilung

NTA

Nanopartikel-Tracking-Analyse (NTA)

NanoSight

Partikelgröße, Größenverteilung und Konzentration

SEC  oder  GPC

Größenausschluss-Chromatographie/

Gelpermeationschromatographie

OMNISEC

Molekülgröße, Molekulargewicht, oligomerer Zustand, Polymer- oder Proteingröße und Molekularstruktur

SPE

Probenvorbereitung durch Schmelzaufschluss

Le Neo

LeDoser

Eagon 2

The OxAdvanced

M4

rFusion

Schmelztabletten-Probenvorbereitung für RFA, Peroxidlösungszubereitungen für ICP, Flussmittelwägung für die Schmelztablettenherstellung

UV/Vis/NIR/ SWIR

Ultraviolett-/Sichtbares Licht-/Nahinfrarot-/Kurzwellen-Infrarotspektrometrie

LabSpec

FieldSpec

TerraSpec

QualitySpec

Materialerkennung und -analyse, Feuchtigkeit, Mineral- und Kohlenstoffgehalt. Bodenuntersuchungen für luft- und satellitengestützte spektroskopische Verfahren.

PFTNA

Aktivierung mit gepulsten schnellen thermischen Neutronen (Pulsed Fast and Thermal Neutron Activation, PFTNA)

CNA

Inline-Elementaranalyse

XRD-C

Röntgendiffraktion  (Kristallographie)

Aeris

Empyrean

Verfeinerung der molekularen Kristallstruktur,

Identifizierung und Quantifizierung der kristallinen Phase, Verhältnis zwischen kristallin und amorph, Analyse der Kristallitgröße

XRD-M

Röntgendiffraktion  (Mikrostruktur)

Empyrean

X’Pert3 MRD(XL)

Eigenspannung, Textur

XRD-CT

Röntgenabsorptionsbildgebung durch Computertomographie

Empyrean

3D Bildgebung von Feststoffen, Porosität und Dichte

SAXS

Kleinwinkel-Röntgenstreuung

Empyrean

Nanopartikel, Größe, Form und Struktur

GISAXS

Kleinwinkel-Röntgenstreuung unter streifendem Einfall

Empyrean

Nanostrukturierte Dünnschichten und Oberflächen

HR-XRD

Hochauflösende Röntgenbeugung

Empyrean

X’Pert3 MRD(XL)

Dünnschichten und epitaktische Mehrfachschichten, Zusammensetzung, Dehnung, Dicke, Qualität

XRR

Röntgenreflektometrie

Empyrean

X’Pert3 MRD(XL)

Dünnschichten und Oberflächen, Schichtdicke, Oberflächen- und Grenzflächenrauheit

RFA

Röntgenfluoreszenz

Epsilon

Zetium

Axios FAST

2830 ZT

Elementzusammensetzung, Elementkonzentration, Spurenelemente, Verunreinigungserkennung