The use of the Empyrean diffractometer in combination with the Oxford Cryostream Plus compact enables us to evaluate the temperature effect on the synthesis process of nanoceria using the small-angle X-ray scattering (SAXS) technique at variable temperatures.

We performed an extensive in situ study of hydrothermal synthesis of nanoceria by combination of X-ray diffraction and scattering techniques. Here we present the results of the in situ SAXS characterization of the nanoceria synthesis process in the temperature range from 5 to 90 °C. 

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