Empyrean Alpha 1

Unrivalled data quality from a laboratory XRD system

The ideal solution for:

  • Solving structures from powder data
  • Searching for polymorphic phases where peak overlap is a hindrance
  • Studying nanomaterial peak profiles to extract crystallite size, dislocation densities, and residual stress
  • Preparing materials for synchrotron beam time

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Overview

Engineered to be the best: Empyrean Alpha 1 is a member of Malvern Panalytical’s family of Empyrean X-ray diffraction systems.

Empyrean Alpha 1 is configured with a unique symmetric Ge monochromator (Johansson type) giving perfect Cu or Co Kα1-only Bragg-Brentano reflection geometry data for structure determination, with unrivaled resolution, excellent peak symmetry, and ultra-low backgrounds - perfect for structural analysis needs.

Thanks to the PreFIX concept on the tube housing, users can easily swap between Kα1-only configuration to Kα1,2 in a matter of minutes.

Om_logo.png   Works with OmniTrust: Malvern Panalytical's compliance solution for the regulated environment

Features

Highest data quality on every sample

Praised by scientists for its performance, Empyrean allows them to prepare for synchrotron beam time in the best possible way. 

The unrivalled collection of sample stages and optical components for Empyrean allows applications to be done in various ways: from ‘simple’ by just adding a few slits and analysis software to a standard geometry, to top performance using dedicated optics, sources and detectors. 

This is ideal for a multipurpose laboratory: if the need for a certain application increases, data quality and throughput time can be improved by adding dedicated modules.

PreFIX

True flexibility for all of your crystallographic needs. 

The key to the Alpha-1’s flexibility is its ingenious use of our PreFIX (Pre-aligned Fast Interchangeable X-ray) technology. This kinematic mounting system is applied to optics, stages and even the tube housing, and allows the diffractometer to be reconfigured in minutes without realignment. 

In five minutes or less, the highresolution Alpha-1 diffractometer becomes a multipurpose diffraction system ready to tackle a variety of analytical challenges.

Multipurpose and future proof

“The only thing constant in life is change”. This holds especially in a research environment, where the analytical needs often change with a redirection of the research program. 

New applications are easily added to an Empyrean system, making it the perfect answer for anything the future holds. 

New and exciting applications are constantly developed on this platform, keeping our customers on the cutting edge of technology.

Hybrid PIXcel technologies

Malvern Panalytical has always been at the forefront of hybrid detector technology. We were the first company to introduce combined 0D and 1D functionality in silicon strip detectors and to expand the onboard flexibility to 0D-1D-2D-3D. 

The small pixel size, zero background and the high dynamic range of our hybrid detectors (PIXcel3D and GaliPIX3D) bring with them a revolution in the way XRD applications are treated. No longer is it necessary to maximize intensity or 2D detector size. 

With a choice of optics and operational radii, you can optimize the configuration to really suit your purpose.

Good laboratory practice

Empyrean with its alignment-free PreFIX modules and measurement and analysis automation possibilities supports anyone who has good laboratory practice (GLP) in mind. 

In addition, every aspect of the Empyrean package, from the hardware to dedicated analysis solutions, comes with extensive tutorials for novice users yet offers access to all functions for experts.

Customized solutions for X-ray diffraction

The Empyrean is a true multi-purpose instrument, designed to support a wide range of applications. Yet, in the market place we often meet scientists and analysts working with our equipment who would like to extend the possibilities even further, according to their own ideas for their own research. 

At Malvern Panalytical, we like to support our users in their materials research. We bring them the right solution for complex analytical problems or cost-effective production processes. 

If you have concepts for new sample holders and stages, optical modules or analytical techniques, discuss your requirements with your local Malvern Panalytical sales representative or submit your request if you need a dedicated solution for your diffraction research. 

Together we can work on advanced solutions for new requirements, keeping pace with the latest developments in the world of science and research.

Well reproducible and highly reliable measurements. Daily work with it is a joy!

Wolfgang Milius — Universität Bayreuth

Specification

Enclosure rating Radiation-safe enclosure with large see-through windows and wide opening doors
Detector type 1Der
PIXcel1D
PIXcel3D
GaliPIX3D
Interface PreFIX type, enabling quick exchange of pre-aligned optics, stages and detectors
Power Supply
Single phase 210 – 230 V (with ± 10% grid variations); 50/60 Hz

Accessories

Detectors

1Der

Ultimate versatility and data clarity in 1D detection

The 1Der is the latest edition to a portfolio of leading solid-state detectors for X-ray diffraction (XRD) applications. Together with an unrivaled suite of optical configurations, the 1Der integrates seamlessly into the XRD platforms to combine ease of use with ultimate flexibility and data clarity for all 0D and 1D applications.

The 1Der is compatible with all X-ray sources that are used on the Empyrean and Aeris.

PIXcel1D

Medipix technology as a dedicated strip detector

With the PIXcel1D detector you have a dedicated strip detector for 0D and 1D applications. You can measure up to 255 times faster than with a traditional point detector, without compromising data quality. With no need for cooling water, liquid nitrogen flow, counting gas or time-consuming calibrations it is a cost-effective solution.

With an unrivalled resolution and dynamic range, the PIXcel1D can be used with all of our diffractometers.

PIXcel3D

The first detector to bring 0D-1D-2D and 3D data to your diffractometer

The PIXcel3D is a unique 2D solid-state hybrid pixel detector. Each pixel is 55 microns x 55 microns and the detector array is 256 x 256 pixels. The detector, now based on Medipix3 technology, brings unrivalled signal to noise with its point spread function of one pixel and multiple energy discrimination levels.

GaliPIX³ᴰ

Extending the range of 2D solid-state pixel detectors

With pixel dimensions of 60 microns x 60 microns and overall sensor dimensions of 30.06 x 24.16 mm, GaliPIX3D is the newest and largest 2D hybrid pixel detector for XRD. The high-quality CdTe sensor provides unrivalled stopping power for X-rays and affords close to 100% efficiency even for the highest energy radiation, like Ag and Mo. As with the PIXcel3D this detector is designed to provide state-of-the-art 2D images, data quality and flexibility. The design of the 2D photon counting detector array allows users to switch seamlessly between 1D and 2D modes and to collect frames suitable for 3D processing in computed tomography.

X-ray tubes

Empyrean Tube

The high-performance X-ray tube

The Empyrean Tube is the successor to Malvern Panalytical’s well-proven X’Pert Tube. Building on the company’s 25 year track record in ceramic tube technology, the Empyrean tube has been designed and optimized for Malvern Panalytical's Empyrean diffractometers. In addition, this state-of-the-art diffraction tube is fully compatible with all Malvern Panalytical’s existing X'Pert PRO, X’Pert Powder, CubiX PRO, CubiX FAST, CubiX³ and X'Pert³ diffractometer systems.

Non-ambient chambers

Non-ambient chambers

We offer a wide range of non-ambient solutions placing ‘in situ’ in front of nearly every application supported on our XRD instruments.

More information
Non-ambient chambers

Software

X-ray diffraction software

Our XRD software packages are designed to extract every bit of information from your material.

More information
X-ray diffraction software

User manuals

Software downloads

Please contact support for the latest software version.

Support

Solutions to maximize the return on your investment

To assure that your instrument remains in top condition and performs on the highest level, Malvern Panalytical offers a wide range of services. Our expertise and support services assure an optimal functioning of your instrument.

Support

Service for a lifetime

  • Phone and remote support
  • Preventive maintenance and checkups
  • Flexible Customer Care Agreements
  • Performance certificates
  • Hardware and software upgrades
  • Local and global support

Expertise

Adding value to your processes 

  • Sample preparation development/optimization
  • Analytical methodologies 
  • Turnkey solutions for XRD 
  • Operations via IQ/OQ/PQ, quality assurance (GLP, ISO17025) or round robins/inter laboratory studies
  • Consultancy services

Training and education

  • Training on-site or at our competence centers
  • Broad range of basic and advanced courses on products, applications and software
Engineered for superior data.

Engineered for superior data.

The Empyrean Alpha 1 offers unrivalled resolution, excellent peak symmetry, and ultra-low background - designed for structural analysis.

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